Extraction Distillation

Extractive distillation is a specialized process used to separate liquid mixtures with components that have very close boiling points, making conventional methods like simple or fractional distillation less effective. It achieves this by introducing a solvent (extracting agent) that changes the relative volatility of the components, allowing for easier separation.

How It Works:

  1. Adding Solvent: A specially chosen solvent is mixed with the liquid to be separated. The solvent alters the boiling behaviour of the components.
  2. Heating: The mixture is heated, and the component with the adjusted boiling point starts to vaporize.
  3. Separation: The vapor is collected, condensed, and separated from the solvent.
  4. Solvent Recovery: The solvent is recycled for reuse, making the process efficient and cost effective.

Applications:

  • Petrochemical Industry: Separation of hydrocarbons with close boiling points, such as in refining processes.
  • Chemical Production: Separation of specialty chemicals or solvents.
  • Pharmaceuticals: Purification of active ingredients and separating complex mixtures.


Benefits:

  • Effective for Difficult Mixtures: Provides separation when boiling points are very close.
  • Energy-Efficient: Requires less energy compared to other methods for such mixtures.
  • Versatile: Can handle various combinations of solvents and components.
  • Cost-Effective: Solvent recovery reduces operational costs.

Material of Construction: SS 304 / SS 316 / MS / As per client needs

Process Flow for Extractive Distillation System

Feed Solution Inlet → (Liquid mixture enters the system for processing)

Solvent Addition Unit → (A specially chosen solvent is mixed with the liquid to
alter component boiling behavior)

Heating Section (Boiler/Reboiler) → (Mixture is heated, initiating selective
vaporization)

Distillation Column
Fractionation Trays / Packing Material → (Ensures effective separation based on
adjusted boiling points)
Co-Current Flow → (Vapor rises, while liquid moves downward with solvent
interaction)

Condenser Unit → (Cools vapor to convert it back into liquid)

Solvent Recovery System → (Extracted solvent is purified and recycled for reuse)

Distillate Collection Tanks → (Separated components are stored for further processing)

Bottoms Outlet → (Residue removed for disposal or additional treatment)

Key Equipment Involved

Feed Pump (Controls liquid entry into the system)

Solvent Injection System (Ensures precise solvent addition for enhanced separation)

Heating Unit (Boiler/Reboiler) (Provides heat for controlled vaporization)

Distillation Column with Packing or Trays (Optimizes fractionation and
component separation)

Condenser Unit (Recovers vapor by converting it into liquid)

Vacuum System (Optional: Reduces boiling point for better efficiency)

Solvent Recovery System (Purifies and reuses solvent for cost-effective operation)

Final Collection Tanks (Stores purified distillate and residue)